Determination of Butenolide (Fusarium Toxin) by Gas Chromatography with an Electron-capture Detector
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منابع مشابه
Determination of Isosorbide Dinitrate in Serum by Gas Chromatography with New Generation of Electron Capture Detector and its Application in Pharmacokinetic Study
Isosorbide dinitrate (ISDN) is an effective drug in treatment of angina pectoris. In this study a new generation of electron capture detector (non-radioactive) with a short, non-polar and wide-bore column was used for analysis of ISDN in human serum. ISDN was extracted from serum by a mixture of ether and ethyl acetate and concentrated at room temperature. The method was linear between 5-50...
متن کاملDetermination of Isosorbide Dinitrate in Serum by Gas Chromatography with New Generation of Electron Capture Detector and its Application in Pharmacokinetic Study
Isosorbide dinitrate (ISDN) is an effective drug in treatment of angina pectoris. In this study a new generation of electron capture detector (non-radioactive) with a short, non-polar and wide-bore column was used for analysis of ISDN in human serum. ISDN was extracted from serum by a mixture of ether and ethyl acetate and concentrated at room temperature. The method was linear between 5-50...
متن کاملDetermination of morphine by electron capture gas-liquid chromatography.
We describe a micromethod for determining as little as 0.1 microgram of morphine per liter of human urine. The procedure is about 20-fold more sensitive than are currently used gas-liquid chromatographic methods. It is particularly suitable for use as a confirmatory method for large-scale radioimmunoassay screening tests. The procedure involves extraction of morphine from urine and analysis of ...
متن کاملDirect acetylation and determination of chlorophenols in aqueous samples by gas chromatography coupled with an electron-capture detector.
A method was developed that offers a rapid, simple and accurate technique for the determination of chlorophenols at trace levels in aqueous samples with very limited volumes of organic solvents. These compounds were acetylated, then preliminarily extracted with n-hexane. The enriched chlorophenols were directly analyzed using gas chromatography with an electron-capture detector. The detection l...
متن کاملDetermination of ethanol in biological samples by gas chromatography with an electron-capture detection.
A simple and sensitive procedure for determination of ethanol in biological samples was established. In this procedure, ethanol in biological samples was first converted to acetaldehyde by yeast alcohol dehydrogenase. Then, acetaldehyde formed was derivatized to 2,4-dinitrophenylhydrazone, which was determined by gas chromatography with an electron-capture detection. Ethanol concentration in 1 ...
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ژورنال
عنوان ژورنال: Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)
سال: 1981
ISSN: 0015-6426,1882-1006
DOI: 10.3358/shokueishi.22.197